|
課程名稱 |
分析化學乙上
Analytical Chemistry (b)(1) |
|
開課學期 |
101-1 |
|
授課對象 |
生物資源暨農學院 森林環境暨資源學系 |
|
授課教師 |
劉春櫻 |
|
課號 |
Chem2011 |
|
課程識別碼 |
203 211B1 |
|
班次 |
|
|
學分 |
2 |
|
全/半年 |
全年 |
|
必/選修 |
必修 |
|
上課時間 |
星期五3,4(10:20~12:10) |
|
上課地點 |
普101 |
|
備註 |
生物材料學群選擇必修，請依指定修習院系班次修習，詳化學系選課須知。
總人數上限：120人 |
|
Ceiba 課程網頁 |
http://ceiba.ntu.edu.tw/1011Chem2011 |
|
課程簡介影片 |
|
|
核心能力關聯 |
本課程尚未建立核心能力關連 |
|
課程大綱
|
|
為確保您我的權利,請尊重智慧財產權及不得非法影印
|
|
課程概述 |
Overview概述: Study of the fundamental principles of quantitative analytical chemistry and their applications
The content of the course includes：
Nature and Tools of Analytical Chemistry
Analytical process
Laboratory tools and techniques
Analytical Measurements
SI units
Chemical concentrations
Reacting unit
Data Handling
Accuracy and precision
Errors and errors propagation
Significant figures
Statistical tests
Q test
Tn test
t test
F test
Measures of central tendency
Measures of variability
Gaussian distribution
Confidence level
Hypothesis test
Detection limits
Least squares method
Standard addition method
Correlation
Stoichiometric Calculations and Chemical equilibrium
Chemical reactions and equilibria
Common ion effect
Activity and activity coefficients
The diverse ion effect
Acid- Base Equilibria and Titrations
Polyprotic acids and their salts
Systematic approach to equilibrium calculations
Titration of polyprotic acids / amino acids
Complexometric Reactions and Titrations
Chelates
EDTA titration and indicators
Auxiliary complexing agents
Precipitation Equilibria and Titrations
Precipitation equilibria
Precipitation titrations
Electrochemical Cells and Potentiometry
Electrodes and reference electrodes
Nernst equation
Formal potential
Liquid junction
Potential measurements
Glass pH electrode
Ion- selective electrodes
Redox titrations
Electroanalytical Techniques
Electrolysis
Coulometry
Voltammetry
|
|
課程目標 |
This course provides students with the background theory and operation principles of chemical analysis methods. The specific objectives of the course are as follows:：
- to become familiar with the various chemical analysis methods currently available
- to develop an understanding of the theories upon which the principles of the common analytical procedures are based
- to understand the correlations of the chemical analysis concepts and of various controllable and measurable quantities
- to learn how the different quantitative analysis methods are used to analyze samples
- to understand the limitations and strengths of particular analysis approaches
- to develop the ability to decide the precision and accuracy of the measurement data by utilizing the necessary mathematical and statistics tools
- to gain skill and competence in the use of analytical standards/references
- to learn to apply chemical equilibria and stoichiometry to solve analytical problems
|
|
課程要求 |
Testing
The exams are primarily problems and short essays, not true-false or multiple choice. They will emphasize the course objectives of understanding the background theory, operation principles, design, applications, strengths, and limitations of the chemical analysis methods introduced. The content of the tests includes the materials discussed in your textbook as well as those taught in the class. The final test is a comprehensive exam and will require you to integrate the class material in a meaningful way. Calculators used in the exam cannot contain any dictionary function. Cell phones and any other communication devices should be kept away from the exam. Anyone who only sits in the class is not allowed to take the midterm or the final.
Make-up policy
Make-up exams will not be permitted to those who miss the midterms or the final. Do not take this course if you have a class/activity schedule that is in some way in conflict with our class and exam schedules. Students should present records of clinic visits for missing the exam due to illness.
Class attendance
Good, participatory attendance is essential to successful mastery of course material. Although the attendance will not be monitored daily, it is suggested that you do not take this course if you cannot come to the class. Handouts are given only in the current class session. Students should keep class notes. Photography and videotaping of any form are not allowed in the classroom.
Honor code
The NTU policies on cheating will be enforced.
|
|
預期每週課後學習時數 |
|
|
Office Hours |
|
|
指定閱讀 |
|
|
參考書目 |
1. Skoog, West, Holler, Crouch, Analytical Chemistry-An Introduction, 7th Ed.,
Thomson, ISBN: 0-03-020293-0
2. Daniel C. Harris, Quantitative Chemical Analysis, 7th Ed., W.H. Freeman and
Company
3. Daniel C. Harris, Exploring Chemical Analysis, W.H. Freeman and Company
4. J. F. Rubinson, K. A. Rubinson, Contemporary Chemical Analysis, Prentice-
Hall, Inc.
5. Gary D. Christian, Analytical Chemistry, 6th Ed., John Wiley & Sons Ltd.,
ISBN: 0-471-45162-2
6. D. A. Skoog, F. J. Holler, S. R. Crouch, Principles of Instrumental
Analysis, 6th Ed., Thomson, ISBN: 0495012017
|
|
評量方式
(僅供參考) |
|
|
週次 |
日期 |
單元主題 |
|
第1週 |
9/14 |
1. Analytical Chemistry-Introduction
2. Tools of the trade (Chapter 2) |
|
第2週 |
9/21 |
Chapter 3 Math toolkit |
|
第3週 |
9/28 |
Chapter 4 Statistics-Part I |
|
第4週 |
10/05 |
Chapter 4 Statistics-Part II |
|
第5週 |
10/12 |
Chapter 5 Quality assurance and calibration methods |
|
第6週 |
10/19 |
Chapter 6 Good titrations |
|
第7週 |
10/26 |
Chapter 7 Gravimetric and combustion analysis |
|
第8週 |
11/02 |
1. 10/26 隨堂考答案
2. Chapter 7 Gravimetric and combustion analysis |
|
第9週 |
11/09 |
期中考 |
|
第10週 |
11/16 |
Chapter 9 Buffers;
Chapter 10 Acid-base titrations |
|
第11週 |
11/23 |
Chapter 11 Polyprotic acids and bases; Reference: Constant boiling HCl
|
|
第12週 |
11/30 |
Chapter 12 A deeper look at chemical equilibrium |
|
第13週 |
12/07 |
Chapter 13 EDTA titrations |
|
第14週 |
12/14 |
Chapter 14 Electrode potentials |
|
第15週 |
12/21 |
Chapter 14 Electrode potentials;
Chapter 15 Electrode potential measurements |
|
第16週 |
12/28 |
Chapter 15 Electrode potential measurements |
|
第17週 |
1/04 |
Chapter 16 Redox titrations |
|