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課程名稱 |
分析化學乙下
Analytical Chemistry (b)(2) |
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開課學期 |
104-2 |
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授課對象 |
生命科學院 生化科技學系 |
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授課教師 |
陳俊顯 |
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課號 |
Chem2012 |
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課程識別碼 |
203 211B2 |
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班次 |
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學分 |
2 |
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全/半年 |
全年 |
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必/選修 |
必修 |
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上課時間 |
星期五3,4(10:20~12:10) |
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上課地點 |
普101 |
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備註 |
請依指定修習院系班次修習。詳化學系選課須知。先修：普化。上下學期需選同一班次。
總人數上限：120人 |
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Ceiba 課程網頁 |
http://ceiba.ntu.edu.tw/1042Chem2012_AC_B |
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課程簡介影片 |
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核心能力關聯 |
本課程尚未建立核心能力關連 |
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課程大綱
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為確保您我的權利,請尊重智慧財產權及不得非法影印
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課程概述 |
Study of the fundamental principles of spectroscopic, spectrometric, and separation analytical chemistry and their applications
This course is presented in a lecture/discussion format. The content of the course includes
Fundamentals of Spectrophotometry
Electromagnetic Radiation
Properties of Light
Absorption and Emission
Absorbance and Transmission
Beer's Law
UV and Visible Molecular Absorption
Infrared Absorption
Luminescence
Flow Injection Analysis
Immunoassays and Aptamers
Spectrophotometers
Lamps and Lasers: Sources of Light
Monochromators
Detectors
Optical Sensors
Surface Plasmon Resonance
Fourier Transform
Mass Spectrometry
Ion Sources
Mass Spectrometers
Mass Spectra
Atomic Spectroscopy
Atomization: Flames, Furnaces, and Plasmas
Temperature Effect
Interference
Inductively Coupled Plasma-Mass Spectroscopy
Analytical Separations
Solvent Extraction
Chromatography
Efficiency of Separation
Bands Spread
Gas Chromatography
Separation Process
Injection and Detection
Detectors
Sample Preparation
High-Performance Liquid Chromatography
Chromatographic Process
Injection and Detection
Reversed-Phase Separations
Gradient Separations
Ion-Exchange Chromatography
Ion Chromatography
Molecular Exclusion Chromatography
Affinity Chromatography
Capillary Electrophoresis
Gravimetric and Combustion Analysis
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課程目標 |
This course provides students with the background theory and operation principles of chemical analysis methods. The specific objectives of the course are as follows:
- to become familiar with the various spectroscopy, spectrometry, and separation methods currently available
- to develop an understanding of the theories upon which the principles of the common spectroscopic, spectrometric, and separation procedures are based
- to understand the correlations of the spectroscopic/spectrometric/separation analysis concepts and of various controllable and measurable quantities
- to learn how the different spectroscopic/spectrometric/separation analysis methods are used to analyze samples
- to understand the limitations and strengths of particular analysis approaches
- to gain skill and competence in the use of related analytical standards/references
- to learn to apply chemical equilibria and stoichiometry to solve spectroscopic/spectrometric/separation analysis problems
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課程要求 |
Good, participatory attendance is essential to successful mastery of course material. Although the attendance will not be monitored daily, it is suggested that you do not take this course if you cannot come to the class. |
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預期每週課後學習時數 |
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Office Hours |
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指定閱讀 |
F. James Holler, Stanley R. Crouch
Skoog and West's Fundamentals of Analytical Chemistry; 9th ed, 2014,
Thomson Brooks/Cole. |
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參考書目 |
1. Harris, D. C.
Quantitative Chemical Analysis; 7th ed, 2007,
W.H. Freeman and Company.
Call number: QD101.2 H37 2007
2. Rouessac, F.; Rouessac, A.
Chemical Analysis:
Modern Instrumentation Methods and Techniques.
2nd ed 2007, John Wiley & Sons.
Call number: QD79.I5 R6813 2007
3. Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Principles of Instrumental Analysis; 6th ed, 1998,
Thomson Brooks/Cole.
Call number: QD79.I5 S58 2007
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評量方式
(僅供參考) |
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No. |
項目 |
百分比 |
說明 |
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1. |
期中考 |
40% |
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2. |
期末考 |
50% |
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3. |
作業 |
10% |
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週次 |
日期 |
單元主題 |
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第1週 |
2/26 |
Introduction to Spectrochemical Methods (Ch 24) |
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第2週 |
3/04 |
Instruments for Optical Spectrometry (Ch 25) |
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第3週 |
3/11 |
Instruments for Optical Spectrometry (Ch 25) |
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第4週 |
3/18 |
Molecular Fluorescence Spectroscopy (Ch 27) |
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第5週 |
3/25 |
Atomic Spec: Atomic Absorption Spectroscopy (Ch 28) |
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第6週 |
4/01 |
Atomic Spec: Atomic Emission Spectroscopy (Ch 28) |
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第7週 |
4/08 |
溫書假/掃墓節連假 |
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第8週 |
4/15 |
Chromatography: intro (Ch 31) |
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第9週 |
4/22 |
mid-term exam (Ch24-28; 佔學期總成績40%)(選擇題的參考答案在右方的 content09.htm；若對答案有其他的想法，請於週日午夜前，將想法/說明以電郵寄至 chhchen@ntu.edu.tw) |
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第10週 |
4/29 |
Chromatography: intro (Ch 31) |
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第11週 |
5/06 |
Chromatography: GC/HPLC (Ch 32) |
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第12週 |
5/13 |
Chromatography: GC/HPLC (Ch 33) |
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第13週 |
5/20 |
Chromatographic Methods & Capillary electrophoresis (Ch 34) |
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第14週 |
5/27這份「內容檔案」是本學期最後一份上課講義；將會使用到第17週結束 |
Mass Spec: ionization methods (Ch 29)我們的Holler的教科書內容過於簡略；這份講義的內容主要來自Harris與Skoog的儀器分析課本。 |
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第15週 |
6/03 |
Mass Spec: mass analyzer (Ch 29) |
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第16週 |
6/04 |
Mass Spec: mass analyzer (Ch 29) 補6/10的彈性放假 |
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第17週 |
6/17 |
Mass Spec: terms & examples (Ch 29) |
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第18週 |
6/24 |
final exam (佔學期總成績50%) (選擇題的參考答案在右方的 content18.htm；若對答案有其他的想法，請於週日午夜前，將想法/說明以電郵寄至 chhchen@ntu.edu.tw，之後便開始閱卷，不再更改答案了。) |
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